DW-XRD-Y3000 XRD Technical Solution

 

I. Brief Description

X-ray diffractometer(XRD) is a widely used large analysis instruments in internal structure of the material studying. It can accurately determine the crystal structure, lattice constant, and complete material qualitative or quantitative analysis. By installing some accessories it can realize structure, macroscopic stress or micro stress determination, crystal size and degree of crystallinity determination, etc., therefore it has have a wide range of applications in the material science, physics, chemistry, chemical engineering, metallurgy, mineral, medicine, building materials, ceramics...And many other disciplines and industries.

 

XRD is a universal test instrument to reveal the crystal structure and chemical information of materials:

l One or more phase identifications in unknown samples;

l Quantitative analysis of known phases in mixed samples;

l Crystal structure analysis;

l The perfect combination of hardware and software can meet the needs of scholars and researchers in different application fields;

l The high precision goniometer system can get more accurate measurement results ;

l By the highly stable X-ray generator control system, it can get more stable repeat measurement precision;

l Programmed operation, integrated structure design, simple operation, and more beautiful instrument appearance.

 

II. DW-XRD-Y3000 XRD Property and Technical Parameter

1.  High pressure generator(Adopting imported PLC control technology):

l Rated Power:3kW;

l Tube Voltage:10~60kV  It is automatically controlled by computer terminal(1kV/step);

l Tube Current:5~80mA  It is automatically controlled by computer terminal(1mA/step);

l Tube Voltage and Current Stability≤0.01%;

l Protection of over voltage, over current, over power, and low water level;

l X-Ray Tube:Cu target,Focal point 1×10mm2,Power 2.0kW; 

l Optical shutter switch is automatically controlled by computer terminal;

l Unibody structure cooling device, Cooling device is unibody structure, and the automatic temperature control system can indicate the water temperature of X-ray tube.

 

1.   Recording and Controlling Unit and Detector:  

l Closed scintillation counter

l Auto differential and integral conversion

l Base line and channel width: 0%~99%

l Continuous adjustable high voltage of detector : 0~2000V

l High voltage stability of detector: ≤0.01%

l Optional X-ray tube target material: Cr,Fe,Co,Cu,Mo

l Energy Spectrum Analysis (Cu,Kα Curve): ≤25%(PC),≤50%(SC)

 

2.   Overall Stability

System overall stability ≤0.3%;

3.   Outline Dimension

XRD host net Dimension:1100×950×1750mm

 

4.   X-ray protection up to national standard

 

5.   On-line control software

     The on-line control software can order the XRD system to do continuous scanning or step

scanning and data acquisition. The software can process the general diffraction data and manage the disk file. Data processing including peak seeking (automatic and manual), single peak integral intensity calculation, smoothing, peak shape amplification, multiple drawing, etc .

 

6.   Application software (English Interface)

8.1  Operation functions:

      Diffraction peak measurement, overlap scanning, net intensity measurement, timer counter, goniometer rotating, goniometer step forward and back, goniometer adjustment, 2θcalibration, tube current and tube voltage optical shutter controlling.

 

8.2  Data analysis and processing function:

8.2.1  Smoothing, background deduction, Kα2 Peeling, peak seeking(mark D value,θvalue, d,2θintensity, half-peak bandwidth, display all parameters and many representing methods of diffraction peak), changing sampling step, eliminating , eliminating miscellaneous peak and Interfering peak, d data and peak position correction.

8.2.2 Calculate integral area, integral breadth, half-peak bandwidth; Spectral graph comparison, map add and subtract, and map combination; Insert text at any location in the map; Two kinds of cursors (small vernier, large cursor);Multiple zoom function; Multiple coordinate modes (linear coordinates, logarithmic coordinates, square coordinates).

8.2.3  Peak amplification: user can make any multiple of any multiple of the map by the left and right keys of the mouse.

 

8.3   Qualitative analysis:

Automatic retrieval and manual retrieval can be performed. Automatic retrieval results include: card number, molecular formula, matching index, reliability factor, and K value. Semi-quantitative analysis and k-value analysis can be carried out.

 

8.4   Quantitative analysis:

The absorption coefficient of the two components is different with the standard addition method, internal standard method and N component absorption coefficient.

 

8.5   The crystallinity of the sub-peak method is calculated

The partial peak process can directly change the parameters of the sub-peak by the mouse, and the difference between the fitting spectrum and the measured spectrum can be seen intuitively.

 

8.6   It can do refinement of cell parameters.

8.7   Index.

8.8  Diffraction data calibration:

          Using standard diffraction data CARDS (1-54 groups), the original data of the measurement was deviated to correct and the instrument measurement error was eliminated.

 

III. DW-XRD-Y3000 XRD Working conditions

1. Host power supply, three-phase five-wire system single 220V (two sets, different phases), each phase current 20A(wire diameter 6mm²), the distribution box has at least 2 sets of air switches above C32 (including one set for computer), the distribution box is no more than 4 meters away from the location of the host;

2.The grounding line resistance ≤4 Ω;

3.The indoor temperature should be kept at 20℃±5℃

4.The power supply circuit shall not be interfered by strong electric equipment;

5.Indoor need to prevent static electricity, dust, shock, noise (less than 50 db);

6.The indoor relative temperature should be controlled below 70% (it is recommended to install air conditioner or dehumidifier);

7.Indoor should have water supply and drainage

 

I V. DW-XRD-Y3000 XRD Configuration List

 

Part	Element	Unit	Qty.
X-Ray High Voltage Generator	1) 1505 High Voltage Transformer	set	1
	2) DW-75kV High Voltage Cable	piece	1
	3) 9850 Control panel	set	1
	4) 9820 High voltage control unit	″	1
	5) 9830 Control gate	″	1
	6) 9810 System Case	″	1
	7) 9840 Main power cable	piece	1
	8) X-ray tube 2kW Cu, Focus size 1×10mm²	piece	1
	9) 3306 Tube holder	set	1
	10) 9924 X-ray Protective cover	″	1
Angle Measuring System	1) 3501 Goniometer	set	1
	2) Goniometer layer board	″	1
	3) Powder sample stage	Set	1
	4) Powder sample plate with blind Holes	piece	20
	5) Powder sample plate with through holes	″	10
	6) Micronutrient powder sample board	″	10
	7) Zero setting sample piece, double-knife edge slit	piece	1
	8) Standard ruler, watch oil	piece	1
	9) Filter  Ni	piece	1
	10) Slit	set	1
Recording and Controlling Unit	1) 2013 Recording and controlling units	set	1
	2) CH132  Scintillation counter	set	1
	3) Counter cable	piece	1
	4) Stepping motor cable	″	2
	5) Interface cable	″	1
Circulating Water Cooling System	1) AL-ZFB-3000 Cooling device	set	1
	2) 9509 Power cable	piece	1
	3) Water pipe 6 meters	piece	2
	4) Water relay cable	piece	1
Computer	1) INTEL Pentium G2030, RAM 2G ,500G Hard disk 19″LCD	set	1
	2) Canon LBP6018 Laser printer	″	1
System Control Program and Applicable Software	1) Data collecting and processing software	piece	1
	2) Data analysis and processing software	″	1
	3) Application software	″	1
	4) Diffraction data card stock	″	1
Technical Material	1) DW-XRD-Y3000 XRD user manual	piece	1
	2) DW-ZFB-3000 Cooling device user manual	″	1
Spare Parts	1) ring rubber blanket	piece	4
	2) Fuse  2A   3A  6A	piece	10

 

 

 

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